Synthesis and Characterization of Some Metal Complexes of

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Awf A.R. Ahmed

Abstract

A new ligand [4-chloro-N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-ylcarb amothioyl) benzamide] (CAP) was synthesized by reaction of P-ChloroBenzoyl isothio cyanate with 4-aminoantipyrine,The ligand was characterized by micro elemental analysis C.H.N.S.,FT-IR,UV-Vis and1H-13CNMR spectra, some transition metals complex of this ligand were prepared and  characterized by FT-IR, UV-Vis spectra, conductivity measurements, magnetic susceptibility and atomic absorption. From the obtained results the molecular formula of all prepared complexes were [M(CAP)2(H2O)2]Cl2(M+2 =Mn, Co, Ni, Cu, Zn, Cd and Hg),the proposed geometrical structure for all complexes were octahedral

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Synthesis and Characterization of Some Metal Complexes of. (2022). Journal of the College of Basic Education, 22(96), 49-62. https://doi.org/10.35950/cbej.v22i96.9014
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pure science articles

How to Cite

Synthesis and Characterization of Some Metal Complexes of. (2022). Journal of the College of Basic Education, 22(96), 49-62. https://doi.org/10.35950/cbej.v22i96.9014

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